Date: Fri, 12 Mar 2010 15:57:00 -0800
Reply-To: DCHAS-L Discussion List <DCHAS-L**At_Symbol_Here**LIST.UVM.EDU>
Sender: DCHAS-L Discussion List <DCHAS-L**At_Symbol_Here**LIST.UVM.EDU>
From: "Debbie M. Decker" <dmdecker**At_Symbol_Here**UCDAVIS.EDU>
Subject: FW: Inactivation of Meta chloro peroxybenzoic acid
Comments: To: Laboratory Safety

Hey all you chemists out there!  I don't quite know where to begin to give 
my colleague, Dexter, advice.

Ideas?

-----Original Message-----
From: Dexter

Debbie
We are using MCPBA to make some epoxides.  I need to purify the MCPBA 
before I use it and the wash and crystalization process leaves a 
significant anoumt in solution.  Usually dichloromethane. I will 
obviuosly discard this solution as toxic waste but I want to deactivate 
the MCPBA that remains.  I have read you can use NaI , ferrous ions, 
potassium hydroxide, sodium thiosulfate, etc.  What in your knowledge is 
the preferred method.  Thanks.   Dexter
-----------------------------

Debbie M. Decker, Campus Chemical Safety Officer
Environmental Health and Safety
University of California, Davis
1 Shields Ave.
Davis, CA=A0 95616
(530)754-7964/(530)752-4527 (FAX)
dmdecker**At_Symbol_Here**ucdavis.edu
Co-Conspirator to Make the World A 
Better Place -- Visit www.HeroicStories.com and join the conspiracy

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